PDF Characterization of Catalytic Materials

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Solid State Chemistry, Surface Chemistry and Catalytic Behaviour
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Heterogeneous Catalytic Materials discusses experimental methods and the latest developments in three areas of research: Catalytic materials are those solids that allow the chemical reaction to occur efficiently and cost-effectively. This book provides you with all necessary information to synthesize, characterize, and relate the properties of a catalyst to its behavior, enabling you to select the appropriate catalyst for the process and reactor system.

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Oxides used both as catalysts and as supports for catalysts , mixed and complex oxides and salts, halides, sulfides, carbides, and unsupported and supported metals are all considered. The book encompasses applications in industrial chemistry, refinery, petrochemistry, biomass conversion, energy production, and environmental protection technologies.

We use cookies to help provide and enhance our service and tailor content and ads. By continuing you agree to the use of cookies. As a first attempt to synthesize WC x nanoparticles, we used planar magnetron sputtering and chemical vapor infiltration CVI. Both yielded satisfactory results albeit the amount of material synthesized by sputtering was limited.

Characterization of catalytic materials - Israel E. Wachs, Lee E. Fitzpatrick - Google Книги

The samples were analyzed by x-ray diffraction for the crystal structure, transmission electron microscope TEM and scanning electron microscope SEM for size determination, Rutherford Backscattering Spectrometry for composition analysis, and x-ray photoelectron spectrometer for the oxidation state analysis. With the two techniques, particles in the range of nm can be prepared.

Introduction to Infrared (IR) Spectroscopy

The Octahedron of Surfaces. The Cuboctahedron of and Surfaces.


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The Open Surface. Catalytic Activity of WC x Nanoparticles. To confirm that the WC x nanoparticles are catalytically active, we tested and compared the dehydrogenation and hydrogenation activities between nano-WC x and supported nanoparticles of Pt.

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Another objective is to determine the feasibility of using nano-WC x as less expensive, more selective catalysts to replace Pt-group metals for the removal of aromatics molecules. The comparison clearly indicates that nano-WC and nano-Pt demonstrate different product selectivity in terms of hydrogenation and dehydrogenation.